Location: Jesser Hall room 131

The Gatan 691 PIPS system is used as the final preparation step for many types of TEM samples. 3 mm disks cut from bulk materials or from embedded cross sections are thinned to less than 50 micron before argon ion milling in the FIB.


PIPS Technique Summary:
 
  •    Up to 6 kV argon ion energy
  •    Rotating sample to provide uniform milling
  •    Two ion guns for milling from top and from bottom
  •    Adjustable beam tilt angles from 2 to 10 degrees incident angle
  •    Ion milling at specific segments during sample rotation for directional ion milling and to protect the sample holder
  •    Suited for conductive and non-conductive samples
PIPS Features:
 
  •    Cryo attachment with liquid nitrogen for sample cooling
  •    Auto termination option when electron tranparency is reached
  •    Optical microscope with digital camera to monitor ion milling progress


Operating manuals and additional information may be found in the Sample Preparation folder on UVa's Sharepoint.

UVA RATES:

 

Gatan 691 Ion Mill Instrument Usage: $17/hr

Gatan 691 Ion Mill Operator Costs:  $60/hr

 

EDUCATIONAL, GOVERNMENT & NON-PROFIT INSTITUTIONS RATES (cost = operator + instrument):

 

Gatan 691 Ion Mill Instrument Usage: $22/hr

Gatan 691 Ion Mill Operator Costs:  $70/hr

 

INDUSTRIAL PARTNER RATES:

 

Gatan 691 Ion Mill Instrument Usage: $30/hr

Gatan 691 Ion Mill Operator Costs:  $125/hr